So, first off, a check valve would have prevented that water coming from the aquarium to the gas separator.
Secondly, if you aren't seeing bubbles in the separator/bubble counter, then your either A)the system isn't sealed properly or B)you didn't correct rehydrate the yeast. 99% of all threads created about problems with DIY CO2 stem from yeast not being activated correctly. If you don't already, get a $2 kitchen thermometer to make sure the water you are rehydrating your yeast in isn't too hot or too cold.