I should have added that you don't use the coke bottle. When I made my solution, I used a graduated cylinder (precise to 1 mL( and a mass scale (accuarate to .05 g). That way I knew it would be accurate.
Sure now you tell me.. LOL
I have also made standards for nitrate, phosphate, and alkalinity. That is how I know my test kits are off.
Have you posted that? That would be a GREAT article to have lying around here!
Again Thanks for the help.